X-ray diffraction (XRD) and x-ray fluorescence (XRF) analysis equipment both generate high intensity ionizing radiation that can cause severe and permanent injury if anybody is exposed to the primary beam even for a few seconds. All persons using x-ray diffraction and analytical devices must register with the Radiation Safety Office and be instructed on the following information.
X-ray Analytical Devices - Standard Operating Procedure
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- Any individual operating or using an x-ray analytical device shall register with the Radiation Safety Office (RSO) and attend a user safety lecture. Only authorized persons shall use x-ray analytical devices.
- Operators and users of x-ray analytical devices shall be provided with a whole-body dosimeter. Each month the RSO will send a new dosimeter for exchange with the previous months.
- A logbook shall be maintained which shall be kept available for inspection by the RSO. The logbook shall contain the following information:
- name of operator or user
- date and time of use
- length of time used
- film badge worn (yes/no)
- A list of authorized persons shall be posted on the analytical device or in the logbook.
- Operators or users shall notify the RSO of any incidents which are suspected to have caused radiation over-exposure.
- In the event that the primary x-ray beam is not intercepted by the experimental apparatus under all conditions of operation, protective measures shall be provided to shield that primary x-ray beam.
- If for any reason it is necessary to temporarily alter safety devices, such as by-passing interlocks or removing shielding, such action shall be:
- dated and posted near the machine so other persons will know of the existing status.
- terminated as soon as possible.
- Unused tube ports shall be closed in such a fashion that accidental radiation exposure will not occur.
Production and Characteristics of X-rays
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- X-rays are produced by bombarding a focus of high-speed electrons on a metal target. As the rapidly moving electrons are suddenly stopped by the metal target, x-rays are produced. (this takes place in an x-ray tube, see attached diagram)
- X-rays are a penetrating form of electromagnetic energy of short-wavelength photons that originate from the electron orbitals.
- Interaction of electrons with the metal target produce 2 main types of x-rays:
- Characteristic
- Bremsstrahlung
Units of Radiation
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MilliRoentgen (mR) is a unit of exposure in air
- 1 R = 87.7 ergs/gm of air
- 1 R = 2.08 x 109 ion pairs/cc of air
- millirem (mrem) is a unit of radiation dose
- 1 R (of low energy x-rays) = 1 rem of radiation dose to tissue
Hazards of Excessive Radiation Exposure
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Symptoms of large amounts of acute whole body radiation exposure:
- 0 - 25 rem ---- no observable effect
- 25 - 50 rem ---- possible blood changes - no serious injury
- 50 - 100 rem -- blood changes - some injury
Dose vs. Effect curve:
- threshold vs. non-threshold
- linear vs. non-linear
Clinical Symptoms of Acute Radiation Over-exposure: (greater than 300 rem)
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- 1 to 3 weeks after over-exposure - erythema, ulceration and blisters
- this may heal during the first month
- then skin may atrophy over the next few months
- after a year - ulceration and blistering may occur because of sun or heat burn
- Amputation may be necessary at dose greater then 10,000 rem
Methods for Controlling Radiation Exposure
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- Time - decrease time, decrease radiation dose (proportional)
- Distance - increase distance, decrease radiation dose (inverse square)
- Shielding - increase shielding, decrease radiation exposure (proportional)
- Signs and labels - decrease accidental radiation exposure
Dosimetry
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Exposure Limits:
NRC annual limit:
- 5 rems - effective dose equivalent (whole body)
- 50 rems - shallow dose equivalent (skin or to each extremity)
- 15 rems - eye dose equivalent (lens of the eye)
- 0.5 rem - dose to embryo/fetus during entire pregnancy
ALARA: As Low as Reasonably Achievable
日韩无码 Dose limits: 10% of the NRC annual limits
Background and other dose levels:
- 295 mrem (millirem) - average background dose in U.S.
- 300 mrem - average dose from 1 abdomen radiograph
- 200 mrem - average dose from 1 dental radiograph
- 20 mrem - average dose from 1 chest radiograph
- 3 mrem - average dose to 日韩无码 personnel in 1 year
Radiation monitoring devices:
- film badge (exchanged every month)
- room monitor (exchanged every month)
- pelvic badge (pregnant radiation workers, exchanged every 2 weeks)
Emergency Procedures
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Working hours call the After working hours or on weekends call 日韩无码 Police Services at ext. 114